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Computational Design of Materials for Organic Photovoltaics Jarvist Moore Frost, Sam Foster, James Kirkpatrick, Thomas Kirchartz, Jenny Nelson Imperial College London [email protected] Originally: MRS Boston Fall 2012 – O8.08 Wednesday 28th November

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Tight Binding - The Hückel Method [[ S J 0. 0. ] [ J S J 0. ] [ 0. J S J ] [ 0. 0. J S ]] H = Hamiltonian very easy to solve Parameters semi-empirical (can derive from DFT) Can treat extremely large systems

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(Boon Kar, 2008) High Mobility Polyfluorine & the β-phase

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PF8 Proposed Structures Grell et al. (Macromolecules 1999, 32, 5810-5817) Chen et al. (Macromolecules 2004, 37, 6833-6838) Planar Zig-Zag [2,1 Helix] Complex Unit Cell [Longer Helix]

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Polyfluorene Copolymers F5 F8 Sumitomo

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Transition Time for Backbone Movements (extracted from MD oligomer simulation, PF8)

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MD Representation → Stiff QM Representation (via Votca) Polyfluorene Tetramer Simulation 250 tetramers – 3.5ns

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Transfer Integrals: PF8 vs. PF5:8 F8-F8-F8-F8 F8-F5-F8-F5

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Predicted Mobility in PF8 vs. PF5:8 cm2 / Vs Simulated Hole Mobilities Simulated Tetramer Densities

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Processing magic → di-octyl Polyfluorene can be persuaded to have high mobilities Samples are glassy Induction of the Beta-phase strongly reduces mobility

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β-Phase α-Phase HOMO Spin Density B3LYP/6-31g* "Formation of the β-phase effectively corresponds to crystallization in one dimension, a remarkably uncommon phenomenon in nature." http://pubs.acs.org/doi/pdfplus/10.1021/nl071207u

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0 1 2 3 4 5 6 7 eV In Vacuum, Beta Phase structures are strained But at accessible energies

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Need larger systems for representative DoS → Python TightBinding http://www.physics.rutgers.edu/pythtb/ Hybrid DFT on Octamers (B3LYP/6-31g* & tuned BNL/6-31g*) - get some trap formation (up to 140 meV)

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50meV Gaussian Site Energy Disorder

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Beta Phase Energetic Trap (5 sites)

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Beta Phase Energetic Trap (10 sites) For Wide Enough trap ~10 sites (no confinement), Trap depth = site Energy change

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P3HT–like polymer (normally flat) A pproxim ate torsional distribution as norm al distribution C onsider beta phase to be sm all pockets of flat regions – (i.e. J is m axim ised is these regions to J0)

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Disordered (torsionally) But FLAT (minima) polymer 70meV

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Polyfluorene–like polymer (Helix / twisted rod) ● Approximate torsional distribution as normal distribution (around 45 degree minima) ● Consider beta phase to be small pockets of flat regions of polymer – (i.e. J is maximised is these regions to J0)

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Disordered (torsionally) TWISTED (~PFO) polymer 596meV

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Conclusions • In polymers, Torsion is important – In P3HT, torsion suffcient to describe DoS – In PFO, natural background twist makes extended regions (Beta phase) deep traps – Traps are not always what one imagines (and be careful what you wish for) Even (or especially?) 1930s electronic-structure techniques can offer useful insights